Localized compression and shear tests on nanotargets with a Berkovich tip and a novel multifunctional tip
Antonio Rinaldi*, P. Peralta, C. Friesen, N. Chawla, Enrico Traversa, K. Sieradzki
This article presents an experimental procedure to perform highly localized compression tests on nanoscale structures/features, such as nanospheres and nanopillars, via standard nanoindentation equipment. Current manufacturing capabilities, such as focused ion beam (FIB), lend themselves well to the creation of micron-spaced nanostructures, but it is fundamental to target an individual instance with little or no damage to the surrounding ones. The procedure successfully addresses the problem of locating and testing purposely designed nanostructures of order of 50 nm or less. The technique is illustrated for the case of closely spaced arrays of nanopillars, which were successfully manufactured, characterized, and tested through several pieces of equipment. For the purposes of compression, along with a traditional Berkovich tip, a new multifunctional (MF) tip was devised. This last tip is endowed with a complex contact geometry enabling both atomic force microscope (AFM) scanning and flat punch compression of the nanostructure. The levels of accuracy in tip positioning as well as robustness to alignment errors are unprecedented in comparison with previous in situ compression tests. As a consequence, the MF tip becomes a versatile tool that can be used beyond uniform compression. As an example, ancillary shear tests in controlled conditions are reported. Such results may lay the bases for metal-forming processes at the nanoscale, such as nanoforging or cutting operations, which are relevant to MEMS design and manufacturing.
Journal of Materials Research
https://doi.org/10.1557/jmr.2009.0099
10.1557/jmr.2009.0099
Dive into the research topics of 'Localized compression and shear tests on nanotargets with a Berkovich tip and a novel multifunctional tip'. Together they form a unique fingerprint.
Nanostructures Chemical Compounds 100%
compression tests Physics & Astronomy 93%
Nanopillars Chemical Compounds 93%
Nanospheres Chemical Compounds 45%
Focused ion beams Chemical Compounds 37%
Nanoindentation Chemical Compounds 32%
Metal forming Chemical Compounds 30%
Rinaldi, A., Peralta, P., Friesen, C., Chawla, N., Traversa, E., & Sieradzki, K. (2009). Localized compression and shear tests on nanotargets with a Berkovich tip and a novel multifunctional tip. Journal of Materials Research, 24(3), 768-775. https://doi.org/10.1557/jmr.2009.0099
Rinaldi, Antonio ; Peralta, P. ; Friesen, C. ; Chawla, N. ; Traversa, Enrico ; Sieradzki, K. / Localized compression and shear tests on nanotargets with a Berkovich tip and a novel multifunctional tip. In: Journal of Materials Research. 2009 ; Vol. 24, No. 3. pp. 768-775.
@article{aef1d93be3794e238837a095cb4b13a5,
title = "Localized compression and shear tests on nanotargets with a Berkovich tip and a novel multifunctional tip",
abstract = "This article presents an experimental procedure to perform highly localized compression tests on nanoscale structures/features, such as nanospheres and nanopillars, via standard nanoindentation equipment. Current manufacturing capabilities, such as focused ion beam (FIB), lend themselves well to the creation of micron-spaced nanostructures, but it is fundamental to target an individual instance with little or no damage to the surrounding ones. The procedure successfully addresses the problem of locating and testing purposely designed nanostructures of order of 50 nm or less. The technique is illustrated for the case of closely spaced arrays of nanopillars, which were successfully manufactured, characterized, and tested through several pieces of equipment. For the purposes of compression, along with a traditional Berkovich tip, a new multifunctional (MF) tip was devised. This last tip is endowed with a complex contact geometry enabling both atomic force microscope (AFM) scanning and flat punch compression of the nanostructure. The levels of accuracy in tip positioning as well as robustness to alignment errors are unprecedented in comparison with previous in situ compression tests. As a consequence, the MF tip becomes a versatile tool that can be used beyond uniform compression. As an example, ancillary shear tests in controlled conditions are reported. Such results may lay the bases for metal-forming processes at the nanoscale, such as nanoforging or cutting operations, which are relevant to MEMS design and manufacturing.",
author = "Antonio Rinaldi and P. Peralta and C. Friesen and N. Chawla and Enrico Traversa and K. Sieradzki",
doi = "10.1557/jmr.2009.0099",
journal = "Journal of Materials Research",
Rinaldi, A, Peralta, P, Friesen, C, Chawla, N, Traversa, E & Sieradzki, K 2009, 'Localized compression and shear tests on nanotargets with a Berkovich tip and a novel multifunctional tip', Journal of Materials Research, vol. 24, no. 3, pp. 768-775. https://doi.org/10.1557/jmr.2009.0099
Localized compression and shear tests on nanotargets with a Berkovich tip and a novel multifunctional tip. / Rinaldi, Antonio; Peralta, P.; Friesen, C.; Chawla, N.; Traversa, Enrico; Sieradzki, K.
In: Journal of Materials Research, Vol. 24, No. 3, 01.03.2009, p. 768-775.
T1 - Localized compression and shear tests on nanotargets with a Berkovich tip and a novel multifunctional tip
AU - Rinaldi, Antonio
AU - Peralta, P.
AU - Friesen, C.
AU - Chawla, N.
AU - Traversa, Enrico
AU - Sieradzki, K.
N2 - This article presents an experimental procedure to perform highly localized compression tests on nanoscale structures/features, such as nanospheres and nanopillars, via standard nanoindentation equipment. Current manufacturing capabilities, such as focused ion beam (FIB), lend themselves well to the creation of micron-spaced nanostructures, but it is fundamental to target an individual instance with little or no damage to the surrounding ones. The procedure successfully addresses the problem of locating and testing purposely designed nanostructures of order of 50 nm or less. The technique is illustrated for the case of closely spaced arrays of nanopillars, which were successfully manufactured, characterized, and tested through several pieces of equipment. For the purposes of compression, along with a traditional Berkovich tip, a new multifunctional (MF) tip was devised. This last tip is endowed with a complex contact geometry enabling both atomic force microscope (AFM) scanning and flat punch compression of the nanostructure. The levels of accuracy in tip positioning as well as robustness to alignment errors are unprecedented in comparison with previous in situ compression tests. As a consequence, the MF tip becomes a versatile tool that can be used beyond uniform compression. As an example, ancillary shear tests in controlled conditions are reported. Such results may lay the bases for metal-forming processes at the nanoscale, such as nanoforging or cutting operations, which are relevant to MEMS design and manufacturing.
AB - This article presents an experimental procedure to perform highly localized compression tests on nanoscale structures/features, such as nanospheres and nanopillars, via standard nanoindentation equipment. Current manufacturing capabilities, such as focused ion beam (FIB), lend themselves well to the creation of micron-spaced nanostructures, but it is fundamental to target an individual instance with little or no damage to the surrounding ones. The procedure successfully addresses the problem of locating and testing purposely designed nanostructures of order of 50 nm or less. The technique is illustrated for the case of closely spaced arrays of nanopillars, which were successfully manufactured, characterized, and tested through several pieces of equipment. For the purposes of compression, along with a traditional Berkovich tip, a new multifunctional (MF) tip was devised. This last tip is endowed with a complex contact geometry enabling both atomic force microscope (AFM) scanning and flat punch compression of the nanostructure. The levels of accuracy in tip positioning as well as robustness to alignment errors are unprecedented in comparison with previous in situ compression tests. As a consequence, the MF tip becomes a versatile tool that can be used beyond uniform compression. As an example, ancillary shear tests in controlled conditions are reported. Such results may lay the bases for metal-forming processes at the nanoscale, such as nanoforging or cutting operations, which are relevant to MEMS design and manufacturing.
U2 - 10.1557/jmr.2009.0099
DO - 10.1557/jmr.2009.0099
JO - Journal of Materials Research
JF - Journal of Materials Research
Rinaldi A, Peralta P, Friesen C, Chawla N, Traversa E, Sieradzki K. Localized compression and shear tests on nanotargets with a Berkovich tip and a novel multifunctional tip. Journal of Materials Research. 2009 Mar 1;24(3):768-775. https://doi.org/10.1557/jmr.2009.0099