  Molecular hydrogen was pressurized in a diamond anvil cell at temperatures
between 5 and 83 K. At a sufficiently high pressure, estimated to be between
477 to 491 GPa, hydrogen became metallic, determined by its reflectance in the
near infrared and fit to a Drude free-electron model. We then studied the
predicted metastability of metallic hydrogen. At a temperature of 5 K the load
on the metallic hydrogen was stepwise reduced until the pressure was zero.
While turning the load or pressure down, the sample evidently transformed to
the molecular phase and escaped; the sample hole closed. We estimate this
pressure to be 113 to 84 GPa. Metallic hydrogen was not observed to be
metastable at zero pressure.
