  We have obtained bulk samples of the graphite intercalation compound, CaC6,
by a novel method of synthesis from highly oriented pyrolytic graphite. The
crystal structure has been completely determined showing that it is the only
member of the MC6, metal-graphite compounds, which has rhombohedral symmetry.
We have clearly shown the occurrence of superconductivity in the bulk sample at
11.5K, using magnetization measurements.
