  Hybrid pixel detectors require a reliable and cost-effective interconnect
technology adapted to the pitch and die sizes of the respective applications.
During the ASIC and sensor R&D phase, and in general for small-scale
applications, such interconnect technologies need to be suitable for the
assembly of single-dies, typically available from Multi-Project-Wafer
submissions. Within the CERN EP R&D programme and the AIDAinnova collaboration,
innovative hybridisation concepts targeting vertex-detector applications at
future colliders are under development. This contribution presents recent
results of a newly developed in-house single-die interconnection process based
on Anisotropic Conductive Film (ACF). The ACF interconnect technology replaces
the solder bumps with conductive particles embedded in an adhesive film. The
electro-mechanical connection between the sensor and the read-out chip is
achieved via thermo-compression of the ACF using a flip-chip device bonder. A
specific pad topology is required to enable the connection via conductive
particles and create cavities into which excess epoxy can flow. This pixel-pad
topology is achieved with an in-house Electroless Nickel Immersion Gold (ENIG)
plating process that is also under development within the project. The ENIG and
ACF processes are qualified with the Timepix3 ASIC and sensors, with 55 um
pixel pitch and 14 um pad diameter. The ACF technology can also be used for
ASIC-PCB/FPC integration, replacing wire bonding or large-pitch solder bumping
techniques. This contribution introduces the ENIG plating and ACF processes and
presents recent results on Timepix3 hybrid assemblies.
