  Electron diffraction and high resolution microscopy have been performed on
Mg1-xAlxB2 with x~0.5. This composition displays a superstructure with a repeat
period of exactly 2c along the c axis and about 10 nm in the a-b plane. The
superstructure results in ring-shaped superreflections in the diffraction
pattern. Irradiation by a strong electron beam results in a loss of the
superstructure and a decrease of about 1% in the c lattice parameter. In-situ
heating and cooling on the other hand showed that the superstructure is stable
from 100 K to 700 K. Possible origins for the superstructure are proposed.
