  Novel BiS2-based superconductors LaO1-xFxBiS2 prepared by the high pressure
synthesis technique were systematically studied. It was found that the high
pressure annealing strongly the lattice as compared to the LaO1-xFxBiS2 samples
prepared by conventional solid state reaction at ambient pressure. Bulk
superconductivity was observed within a wide F-concentration range of x = 0.2 ~
0.7. On the basis of those results, we have established a phase diagram of
LaO1-xFxBiS2.
